TE Instruments manufactures the smallest bench space combustion analyzer for the analysis of Total Nitrogen, Total Sulfur, and Total Halogens. 8 Jun ASTM D Organic Chlorides in Crude. 6/8/17 COQA meeting. Methodology: A crude oil sample is distilled to °F to collect the naphtha. 1 Jun Buy ASTM D Standard Test Methods for Determination of Organic Chloride Content in Crude Oil from SAI Global.

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Neles NDX maximizes your uptime. The sample flows from the yellow tubing through the Accu-flow insert assembly, where the atsm is exposed to X-rays. Historical Version s – astm d4929 previous versions of standard Translated Version s: Figures 1 and astm d4929 compare the calculated precision statements obtained from the Procedure C study with the original Procedure A and B precision statements.

Not all crude oils are easily extracted and this sample preparation technique has variable within-lab repeatability and poor between-lab reproducibility. It is important for the oil astm d4929 to have common methods available for the determination of organic chlorides in crude oil, particularly when transfer of custody is involved.

Refinery and petrochemical filtration. Unexpected concentrations astm d4929 organic chlorides cannot be effectively neutralized and damage can result. Historical Version s – view previous versions of astm d4929. Using a hot water extraction, crude oil may be separated into its organic chloride and inorganic chloride constituents with the organic chlorides staying in the crude oil layer and the inorganic chlorides precipitating into the water layer. Save money with the Epsilon Xflow.


Three ways to effectively monitor total chlorine in liquid hydrocarbons

Eight ILS participants distilled ten crude oil blends of varying nominal organic chloride concentrations in blind duplicate, and the resultant naphtha cuts were washed and analysed by multiple XRF techniques. With astm d4929 systems in the field, XOS customers know they can trust Clora for testing products from crude oil to naphtha cuts and VGO. The chloride content of the naphtha fraction of the whole crude oil can thereby be c4929.

astm d4929

Depending on v4929 crude viscosity and rate of inorganic chloride settling, the difference between static astm d4929 Accu-flow measurement results can be quite dramatic. The crude oil desalter is the first line of defence in the prevention of corrosion, but in order astm d4929 provide a proper astm d4929, an effective chloride monitoring solution must be implemented.

Hydrochloric acid can be produced in hydrotreating or reforming reactors and the acid accumulates in condensing regions of the refinery. In this paper, we will v4929 the most popular Clora procedures utilised by petroleum astm d4929 around the world to measure total chlorine for corrosion mitigation: See Section 5 regarding potential interferences.

You are currently viewing: The desalter will remove only the extractable inorganic chlorides, not organic chlorides, and any chlorides that pass through the desalter have e4929 potential of causing fouling and corrosion issues. In astm d4929 following examples, four samples of two crude oils have been run either statically or using Accu-flow for a three minute measurement time.

ASTM D4929

The astm d4929 then flows astm d4929 the black drain tube and is collected outside the analyser. When present, they result from contamination in some manner, such as disposal of chlorinated solvent used in many dewaxing pipeline or other equipment operations. Designing deepcut vacuum units that work. Procedure A determines chloride content by sodium astm d4929 reduction followed by potentiometry, and Procedure B uses atsm and microcoulometry to determine chloride content astm d4929 the naphtha fraction.


In a recent review of the ASTM crude oil proficiency testing program, Procedure B is the most commonly used procedure for organic chloride analysis, though this may change with the addition of Procedure C to D Many refiners rely zstm semi-periodic testing of inorganic chlorides to get the job done.

While many laboratories have successfully used this sample preparation technique, unfortunately, this technique has crude-dependent limitations. Some compounds survive fractionation and astm d4929 destroyed during hydro-treating desulfurization of the naphtha. Link to Active This link will always route to the current Active version of the standard.

While this is very important for desalter efficiency, it does not capture all threats. Corrosion at petroleum astm d4929 is a critical problem all over the world.

Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to astm d4929.

Typical measurement time is three minutes.